色譜條件 |
色譜柱 |
流動(dòng)相 |
波長(zhǎng)nm |
柱溫 |
保留時(shí)間min |
進(jìn)樣量 |
流速ml/min |
Astragaloside IV |
Nucleosil 5 C-18(4.6X25cm) |
乙腈-水(1:2) |
200 |
室溫 |
|
20μl |
0.8 |
Ciwujianoside B |
ODS(4.6mmX25cm) |
甲醇-水(9:1) |
203 |
|
5.5 |
|
0.7 |
Gastrodin |
YWG-C18,10μm(4.6mmX25cm) |
甲醇-水(30:70) |
270 |
室溫 |
7.7 |
|
0.7 |
Ginsenoside Rb1 |
YWG-C18,10μm(4.6mmX25cm) |
甲醇-水(74:26) |
205 |
|
10 |
|
1.0 |
Ginsenoside Rg1 |
KYWG-C18,10μm(4.6mmX25cm) |
甲醇-水(59:41) |
203 |
|
|
|
7.8 |
Icariin |
YWG-C18,10μm(4.6mmX25cm) |
甲醇-水-醋酸(60:40:0.5) |
270 |
|
11.1 |
|
1.2 |
Loganin |
大連依利特hypersil C18,5μm(4.6mmX25cm) |
乙腈-0.05%磷酸二氫鈉(15:85) |
237 |
|
|
|
1 |
Osthol |
LC-4A ZorbaxODS(Dupont)(4.6mmX25cm) |
(1)甲醇-水(67:33);(2)甲醇-水-四氫呋喃(53:42:5) |
249 |
|
|
|
0.8 |
Paeoniflorin |
YWG-C18 ODS5μm(4.6mmX25cm) |
乙腈-水(15:85) |
230 |
|
|
|
1.0 |
Saikosaponin a |
YWC ODS A-311(6mmX10cm) |
乙腈-水(35:65) |
203 |
40℃ |
|
|
3.0 |
Schizandrin |
LS-120A(4.6X25cm,10μm) |
乙腈-水(1:1) |
252 |
25℃ |
|
|
1.0 |
Tanshinone I |
NucleosilC18(4.6mmX25cm,510μm) |
77.5%甲醇水溶液 |
|
|
|
|
|
Tanshinone IIA |
|
|
|
|
|
|
|
Tetrandrin |
C18反向柱 |
甲醇:水=70:30,加少許三乙銨 |
254 |
|
|
|
1.0 |